TY - JOUR
T1 - 4-Amino-5-methyl-1,2,4-triazole-3-thione derivative of 4-[2-(2 hydroxyethyl)methylamino]benzaldehyde
AU - Wu, Ji
AU - Tian, Yu-Peng
AU - Xie, Fu-Xin
AU - Chantrapromma, Suchada
AU - Fun, Hoong-Kun
AU - Razak, Ibrahim Abdul
N1 - Refinement. Refinement of F 2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F 2, conventional R-factors R are based on F, with F set to zero for negative F 2. The threshold expression of F 2 > σ( F 2) is used only for calculating R-factors(gt) etc.
PY - 2001
Y1 - 2001
N2 - The title compound, 4-{4-[2-(2-hydroxyethyl)methylamino]benzylideneamino}-5-methyl-1,2,4-triazole-3-thione, C13H17N5OS, is present in a thioketone form and the triazole ring is almost planar. The asymmetric unit consists of two molecules which have different conformations. There is a weak C-H...S intramolecular interaction, a weak O-H...S intermolecular interaction and intermolecular N-H...O and O-H...N hydrogen bonds.
AB - The title compound, 4-{4-[2-(2-hydroxyethyl)methylamino]benzylideneamino}-5-methyl-1,2,4-triazole-3-thione, C13H17N5OS, is present in a thioketone form and the triazole ring is almost planar. The asymmetric unit consists of two molecules which have different conformations. There is a weak C-H...S intramolecular interaction, a weak O-H...S intermolecular interaction and intermolecular N-H...O and O-H...N hydrogen bonds.
KW - 2
KW - 4-Amino-5-methyl-1
KW - 4-[2-(2 hydroxyethyl)methylamino]benzaldehyde
KW - 4-triazole-3-thione derivative
UR - https://doi.org/10.1107/S1600536801007851
U2 - 10.1107/S1600536801007851
DO - 10.1107/S1600536801007851
M3 - Article
VL - E57
JO - Acta Crystallographica, Section E
JF - Acta Crystallographica, Section E
ER -