A Solvent-Reduction Approach to Tetrapod-Like Copper(I) Chloride Crystallites

Qing Li; Mingwang Shao; Guihua Yu; Ji Wu; Fanqing Li; Yitai Qian

doi:10.1039/B204858B

A Solvent-Reduction Approach to Tetrapod-Like Copper(I) Chloride Crystallites

Qing Li, Mingwang Shao, Guihua Yu, Ji Wu, Fanqing Li, Yitai Qian

Biochemistry, Chemistry, & Physics

University of Science and Technology of China

Research output: Contribution to journal › Article › peer-review

17 Scopus citations

Abstract

Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120 °C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV–Vis and PL techniques. The average length of the legs of T-CuCl is 30 µm. The morphologies of the products were related to the reaction temperature, time and the volume ratio of the solvents. A solvent-mediated morphological transformation mechanism was proposed and it was in good agreement with the observations made with scanning electron microscopy. The role of the two solvents was also explored.

Original language	American English
Journal	Journal of Materials Chemistry
Volume	13
DOIs	https://doi.org/10.1039/B204858B
State	Published - 2003

Keywords

chloride
copper(I)
crystallites
solvent-reduction
tetrapod-like

DC Disciplines

Chemistry

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title = "A Solvent-Reduction Approach to Tetrapod-Like Copper(I) Chloride Crystallites",

abstract = " Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120 °C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV–Vis and PL techniques. The average length of the legs of T-CuCl is 30 µm. The morphologies of the products were related to the reaction temperature, time and the volume ratio of the solvents. A solvent-mediated morphological transformation mechanism was proposed and it was in good agreement with the observations made with scanning electron microscopy. The role of the two solvents was also explored.",

keywords = "chloride, copper(I), crystallites, solvent-reduction, tetrapod-like",

author = "Qing Li and Mingwang Shao and Guihua Yu and Ji Wu and Fanqing Li and Yitai Qian",

note = "Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120 °C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV-Vis and PL techniques. The average length of the legs of T-CuCl is 30 µm. The m",

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doi = "10.1039/B204858B",

language = "American English",

volume = "13",

journal = "Journal of Materials Chemistry",

issn = "0959-9428",

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TY - JOUR

T1 - A Solvent-Reduction Approach to Tetrapod-Like Copper(I) Chloride Crystallites

AU - Li, Qing

AU - Shao, Mingwang

AU - Yu, Guihua

AU - Wu, Ji

AU - Li, Fanqing

AU - Qian, Yitai

N1 - Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120 °C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV-Vis and PL techniques. The average length of the legs of T-CuCl is 30 µm. The m

PY - 2003

Y1 - 2003

N2 - Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120 °C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV–Vis and PL techniques. The average length of the legs of T-CuCl is 30 µm. The morphologies of the products were related to the reaction temperature, time and the volume ratio of the solvents. A solvent-mediated morphological transformation mechanism was proposed and it was in good agreement with the observations made with scanning electron microscopy. The role of the two solvents was also explored.

AB - Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120 °C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV–Vis and PL techniques. The average length of the legs of T-CuCl is 30 µm. The morphologies of the products were related to the reaction temperature, time and the volume ratio of the solvents. A solvent-mediated morphological transformation mechanism was proposed and it was in good agreement with the observations made with scanning electron microscopy. The role of the two solvents was also explored.

KW - chloride

KW - copper(I)

KW - crystallites

KW - solvent-reduction

KW - tetrapod-like

UR - https://doi.org/10.1039/B204858B

U2 - 10.1039/B204858B

DO - 10.1039/B204858B

M3 - Article

SN - 0959-9428

VL - 13

JO - Journal of Materials Chemistry

JF - Journal of Materials Chemistry

ER -

A Solvent-Reduction Approach to Tetrapod-Like Copper(I) Chloride Crystallites

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