A solvent-reduction approach to tetrapod-like copper(I) chloride crystallites

Qing Li; Mingwang Shao; Guihua Yu; Ji Wu; Fanqing Li; Yitai Qian

doi:10.1039/b204858b

A solvent-reduction approach to tetrapod-like copper(I) chloride crystallites

Qing Li, Mingwang Shao, Guihua Yu, Ji Wu, Fanqing Li, Yitai Qian

Biochemistry, Chemistry & Physics

University of Science and Technology of China

Research output: Contribution to journal › Article › peer-review

17 Scopus citations

Abstract

Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120°C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV-Vis and PL techniques. The average length of the legs of T-CuCl is 30 μm. The morphologies of the products were related to the reaction temperature, time and the volume ratio of the solvents. A solution-mediated morphological transformation mechanism was proposed and it was in good agreement with the observations made with scanning electron microscopy. The role of the two solvents was also explored.

Original language	English
Pages (from-to)	424-427
Number of pages	4
Journal	Journal of Materials Chemistry
Volume	13
Issue number	2
DOIs	https://doi.org/10.1039/b204858b
State	Published - Feb 1 2003

Scopus Subject Areas

General Chemistry
Materials Chemistry

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10.1039/b204858b

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title = "A solvent-reduction approach to tetrapod-like copper(I) chloride crystallites",

abstract = "Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120°C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV-Vis and PL techniques. The average length of the legs of T-CuCl is 30 μm. The morphologies of the products were related to the reaction temperature, time and the volume ratio of the solvents. A solution-mediated morphological transformation mechanism was proposed and it was in good agreement with the observations made with scanning electron microscopy. The role of the two solvents was also explored.",

author = "Qing Li and Mingwang Shao and Guihua Yu and Ji Wu and Fanqing Li and Yitai Qian",

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T1 - A solvent-reduction approach to tetrapod-like copper(I) chloride crystallites

AU - Li, Qing

AU - Shao, Mingwang

AU - Yu, Guihua

AU - Wu, Ji

AU - Li, Fanqing

AU - Qian, Yitai

N1 - Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120 °C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV-Vis and PL techniques. The average length of the legs of T-CuCl is 30 µm. The m

PY - 2003/2/1

Y1 - 2003/2/1

N2 - Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120°C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV-Vis and PL techniques. The average length of the legs of T-CuCl is 30 μm. The morphologies of the products were related to the reaction temperature, time and the volume ratio of the solvents. A solution-mediated morphological transformation mechanism was proposed and it was in good agreement with the observations made with scanning electron microscopy. The role of the two solvents was also explored.

AB - Tetrapod-like CuCl crystallites with uniform sizes were generated conveniently in a mixed solution of acetylacetone and ethylene glycol at 120°C under solvothermal conditions. The products were characterized by XRD, XPS, SEM, UV-Vis and PL techniques. The average length of the legs of T-CuCl is 30 μm. The morphologies of the products were related to the reaction temperature, time and the volume ratio of the solvents. A solution-mediated morphological transformation mechanism was proposed and it was in good agreement with the observations made with scanning electron microscopy. The role of the two solvents was also explored.

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U2 - 10.1039/b204858b

DO - 10.1039/b204858b

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EP - 427

JO - Journal of Materials Chemistry

JF - Journal of Materials Chemistry

IS - 2

ER -

A solvent-reduction approach to tetrapod-like copper(I) chloride crystallites

Abstract

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A solvent-reduction approach to tetrapod-like copper(I) chloride crystallites

Abstract

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Scanning Electron Microscope - JEOL JSM-7600F

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