Biphenyl-3-carboxylic acid at 296 and 203 K

Allison J. Amonette; A.C. Blackburn; Roger E. Gerkin

doi:10.1107/S0108270196003514

Biphenyl-3-carboxylic acid at 296 and 203 K

Allison J. Amonette
, A.C. Blackburn
, Roger E. Gerkin

Biochemistry, Chemistry & Physics

Ohio State University

Research output: Contribution to journal › Article › peer-review

7 Scopus citations

Abstract

In biphenyl-3-carboxylic acid, C 13 H 10 O 2 , hydrogen bonding is of the cyclic dimer type about a center of symmetry. The carboxyl H atom is ordered. The dihedral angle between the planar phenyl rings is 31.78 (8)° at 296 K and 31.27 (6)° at 203 K. The data show that the larger than average magnitudes of the displacement parameters of the carboxylic O atoms are due to thermal motion rather than static disorder.

Original language	English
Pages (from-to)	2320-2323
Number of pages	4
Journal	Acta Crystallographica Section C: Crystal Structure Communications
Volume	52
Issue number	9
DOIs	https://doi.org/10.1107/S0108270196003514
State	Published - Sep 15 1996

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General Biochemistry, Genetics and Molecular Biology

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@article{7a85d7ddda5a4ff3a60ac6b4e6d9c310,

title = "Biphenyl-3-carboxylic acid at 296 and 203 K",

abstract = " In biphenyl-3-carboxylic acid, C 13 H 10 O 2 , hydrogen bonding is of the cyclic dimer type about a center of symmetry. The carboxyl H atom is ordered. The dihedral angle between the planar phenyl rings is 31.78 (8)° at 296 K and 31.27 (6)° at 203 K. The data show that the larger than average magnitudes of the displacement parameters of the carboxylic O atoms are due to thermal motion rather than static disorder. ",

author = "Amonette, \{Allison J.\} and A.C. Blackburn and Gerkin, \{Roger E.\}",

note = "In biphenyl-3-carboxylic acid, CHO, hydrogen bonding is of the cyclic dimer type about a center of symmetry. The carboxyl H atom is ordered. The dihedral angle between the planar phenyl rings is 31.78 (8)° at 296 K and 31.27 (6)° at 203 K.",

year = "1996",

month = sep,

day = "15",

doi = "10.1107/S0108270196003514",

language = "English",

volume = "52",

pages = "2320--2323",

journal = "Acta Crystallographica Section C: Crystal Structure Communications",

issn = "0108-2701",

publisher = "International Union of Crystallography",

number = "9",

}

TY - JOUR

T1 - Biphenyl-3-carboxylic acid at 296 and 203 K

AU - Amonette, Allison J.

AU - Blackburn, A.C.

AU - Gerkin, Roger E.

N1 - In biphenyl-3-carboxylic acid, CHO, hydrogen bonding is of the cyclic dimer type about a center of symmetry. The carboxyl H atom is ordered. The dihedral angle between the planar phenyl rings is 31.78 (8)° at 296 K and 31.27 (6)° at 203 K.

PY - 1996/9/15

Y1 - 1996/9/15

N2 - In biphenyl-3-carboxylic acid, C 13 H 10 O 2 , hydrogen bonding is of the cyclic dimer type about a center of symmetry. The carboxyl H atom is ordered. The dihedral angle between the planar phenyl rings is 31.78 (8)° at 296 K and 31.27 (6)° at 203 K. The data show that the larger than average magnitudes of the displacement parameters of the carboxylic O atoms are due to thermal motion rather than static disorder.

AB - In biphenyl-3-carboxylic acid, C 13 H 10 O 2 , hydrogen bonding is of the cyclic dimer type about a center of symmetry. The carboxyl H atom is ordered. The dihedral angle between the planar phenyl rings is 31.78 (8)° at 296 K and 31.27 (6)° at 203 K. The data show that the larger than average magnitudes of the displacement parameters of the carboxylic O atoms are due to thermal motion rather than static disorder.

UR - https://www.scopus.com/pages/publications/0030242693

U2 - 10.1107/S0108270196003514

DO - 10.1107/S0108270196003514

M3 - Article

SN - 0108-2701

VL - 52

SP - 2320

EP - 2323

JO - Acta Crystallographica Section C: Crystal Structure Communications

JF - Acta Crystallographica Section C: Crystal Structure Communications

IS - 9

ER -

Biphenyl-3-carboxylic acid at 296 and 203 K

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