Bis(pyridinium) pamoate

A.C. Blackburn; Allison J. Amonette; Roger E. Gerkin

doi:10.1107/S0108270195015691

Bis(pyridinium) pamoate

A.C. Blackburn
, Allison J. Amonette
, Roger E. Gerkin

Biochemistry, Chemistry & Physics

Ohio State University

Research output: Contribution to journal › Article › peer-review

13 Scopus citations

Abstract

Attempted crystallization of pamoic acid from its solution in pyridine instead produced the crystalline title compound, bis(pyridinium) 4,4'-methylenebis(3-hydroxy-2-naphthalenecarboxylate), 2C 5 H 6 N + .C 23 H 14 O 62- . In this structure, intramolecular hydrogen bonding involves hydroxyl O atoms as donors and carboxylate O atoms as acceptors, while intermolecular hydrogen bonds involve N atoms as donors and carboxylate O atoms as acceptors. Each N atom and each O atom participates in a strong hydrogen bond. The H atoms involved in hydrogen bonding are ordered.

Original language	English
Pages (from-to)	1269-1272
Number of pages	4
Journal	Acta Crystallographica Section C: Crystal Structure Communications
Volume	52
Issue number	5
DOIs	https://doi.org/10.1107/S0108270195015691
State	Published - May 15 1996

Scopus Subject Areas

General Biochemistry, Genetics and Molecular Biology

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title = "Bis(pyridinium) pamoate",

abstract = " Attempted crystallization of pamoic acid from its solution in pyridine instead produced the crystalline title compound, bis(pyridinium) 4,4'-methylenebis(3-hydroxy-2-naphthalenecarboxylate), 2C 5 H 6 N + .C 23 H 14 O 62- . In this structure, intramolecular hydrogen bonding involves hydroxyl O atoms as donors and carboxylate O atoms as acceptors, while intermolecular hydrogen bonds involve N atoms as donors and carboxylate O atoms as acceptors. Each N atom and each O atom participates in a strong hydrogen bond. The H atoms involved in hydrogen bonding are ordered. ",

author = "A.C. Blackburn and Amonette, \{Allison J.\} and Gerkin, \{Roger E.\}",

note = "Attempted crystallization of pamoic acid from its solution in pyridine instead produced the crystalline title compound, bis(pyridinium) 4,4'-methylenebis(3-hydroxy-2-naphthalenecarboxylate), 2CHN.CHO. In this structure, intramolecular hydrogen bonding involves hydroxyl O atoms as donors and carboxylate O atoms as acceptors, while intermolecular hydrogen bonds involve N atoms as donors and carboxylate O atoms as acceptors.",

year = "1996",

month = may,

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doi = "10.1107/S0108270195015691",

language = "English",

volume = "52",

pages = "1269--1272",

journal = "Acta Crystallographica Section C: Crystal Structure Communications",

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publisher = "International Union of Crystallography",

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T1 - Bis(pyridinium) pamoate

AU - Blackburn, A.C.

AU - Amonette, Allison J.

AU - Gerkin, Roger E.

N1 - Attempted crystallization of pamoic acid from its solution in pyridine instead produced the crystalline title compound, bis(pyridinium) 4,4'-methylenebis(3-hydroxy-2-naphthalenecarboxylate), 2CHN.CHO. In this structure, intramolecular hydrogen bonding involves hydroxyl O atoms as donors and carboxylate O atoms as acceptors, while intermolecular hydrogen bonds involve N atoms as donors and carboxylate O atoms as acceptors.

PY - 1996/5/15

Y1 - 1996/5/15

N2 - Attempted crystallization of pamoic acid from its solution in pyridine instead produced the crystalline title compound, bis(pyridinium) 4,4'-methylenebis(3-hydroxy-2-naphthalenecarboxylate), 2C 5 H 6 N + .C 23 H 14 O 62- . In this structure, intramolecular hydrogen bonding involves hydroxyl O atoms as donors and carboxylate O atoms as acceptors, while intermolecular hydrogen bonds involve N atoms as donors and carboxylate O atoms as acceptors. Each N atom and each O atom participates in a strong hydrogen bond. The H atoms involved in hydrogen bonding are ordered.

AB - Attempted crystallization of pamoic acid from its solution in pyridine instead produced the crystalline title compound, bis(pyridinium) 4,4'-methylenebis(3-hydroxy-2-naphthalenecarboxylate), 2C 5 H 6 N + .C 23 H 14 O 62- . In this structure, intramolecular hydrogen bonding involves hydroxyl O atoms as donors and carboxylate O atoms as acceptors, while intermolecular hydrogen bonds involve N atoms as donors and carboxylate O atoms as acceptors. Each N atom and each O atom participates in a strong hydrogen bond. The H atoms involved in hydrogen bonding are ordered.

UR - https://www.scopus.com/pages/publications/0030145704

U2 - 10.1107/S0108270195015691

DO - 10.1107/S0108270195015691

M3 - Article

SN - 0108-2701

VL - 52

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EP - 1272

JO - Acta Crystallographica Section C: Crystal Structure Communications

JF - Acta Crystallographica Section C: Crystal Structure Communications

IS - 5

ER -

Bis(pyridinium) pamoate

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