Hydrogen Bonding and C-H---O Interactions In 3-(3-Aminophthalimido)-Phthalic Acid Dihydrate

Allison J. Amonette; Roger E. Gerkin

doi:10.1107/S0108270100007083

Hydrogen Bonding and C-H---O Interactions In 3-(3-Aminophthalimido)-Phthalic Acid Dihydrate

Allison J. Amonette, Roger E. Gerkin

Emeriti, Retired, & In Memoriam (COSM)

Ohio State University

Research output: Contribution to journal › Article › peer-review

Abstract

The title compound, C ₁₆ H ₁₀ N ₂ O _6· 2H ₂ O, crystallized in the centrosymmetric triclinic space group P1 with one organic molecule and two water molecules as the asymmetric unit. Eight intermolecular hydrogen bonds have donoracceptor distances in the range 2.602 (2)-3.289 (2) Å, with angles in the range 137 (2)-177 (2)°. These generate a three-dimensional hydrogen-bond network. There is a single intramolecular hydrogen bond. There are six significant intermolecular C-HO interactions with HO distances in the range 2.39-2.74 Å, and C-HO angles in the range 131-157°.

Original language	American English
Journal	Acta Crystallographica
Volume	C56
DOIs	https://doi.org/10.1107/S0108270100007083
State	Published - Jan 1 2000

Keywords

Hydrogen bonding

DC Disciplines

Chemistry

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title = "Hydrogen Bonding and C-H---O Interactions In 3-(3-Aminophthalimido)-Phthalic Acid Dihydrate",

abstract = " The title compound, C 16 H 10 N 2 O 6· 2H 2 O, crystallized in the centrosymmetric triclinic space group P1 with one organic molecule and two water molecules as the asymmetric unit. Eight intermolecular hydrogen bonds have donoracceptor distances in the range 2.602 (2)-3.289 (2) {\AA}, with angles in the range 137 (2)-177 (2)°. These generate a three-dimensional hydrogen-bond network. There is a single intramolecular hydrogen bond. There are six significant intermolecular C-HO interactions with HO distances in the range 2.39-2.74 {\AA}, and C-HO angles in the range 131-157°.",

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year = "2000",

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T1 - Hydrogen Bonding and C-H---O Interactions In 3-(3-Aminophthalimido)-Phthalic Acid Dihydrate

AU - Amonette, Allison J.

AU - Gerkin, Roger E.

PY - 2000/1/1

Y1 - 2000/1/1

N2 - The title compound, C 16 H 10 N 2 O 6· 2H 2 O, crystallized in the centrosymmetric triclinic space group P1 with one organic molecule and two water molecules as the asymmetric unit. Eight intermolecular hydrogen bonds have donoracceptor distances in the range 2.602 (2)-3.289 (2) Å, with angles in the range 137 (2)-177 (2)°. These generate a three-dimensional hydrogen-bond network. There is a single intramolecular hydrogen bond. There are six significant intermolecular C-HO interactions with HO distances in the range 2.39-2.74 Å, and C-HO angles in the range 131-157°.

AB - The title compound, C 16 H 10 N 2 O 6· 2H 2 O, crystallized in the centrosymmetric triclinic space group P1 with one organic molecule and two water molecules as the asymmetric unit. Eight intermolecular hydrogen bonds have donoracceptor distances in the range 2.602 (2)-3.289 (2) Å, with angles in the range 137 (2)-177 (2)°. These generate a three-dimensional hydrogen-bond network. There is a single intramolecular hydrogen bond. There are six significant intermolecular C-HO interactions with HO distances in the range 2.39-2.74 Å, and C-HO angles in the range 131-157°.

KW - Hydrogen bonding

UR - https://digitalcommons.georgiasouthern.edu/chem-facpubs/8

UR - http://dx.doi.org/10.1107/S0108270100007083

U2 - 10.1107/S0108270100007083

DO - 10.1107/S0108270100007083

M3 - Article

SN - 0365-110X

VL - C56

JO - Acta Crystallographica

JF - Acta Crystallographica

ER -

Hydrogen Bonding and C-H---O Interactions In 3-(3-Aminophthalimido)-Phthalic Acid Dihydrate

Abstract

Keywords

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