Hydrogen bonding and C-H⋯O interactions in 3-(3-aminophthalimido)phthalic acid dihydrate

Allison J. Amonette; Roger E. Gerkin

doi:10.1107/s0108270100007083

Hydrogen bonding and C-H⋯O interactions in 3-(3-aminophthalimido)phthalic acid dihydrate

Allison J. Amonette, Roger E. Gerkin

Biochemistry, Chemistry & Physics

Ohio State University

Research output: Contribution to journal › Article › peer-review

Abstract

The title compound, C16H10N2O6-2H2O, crystallized in the centrosymmetric triclinic space group PI with one organic molecule and two water molecules as the asymmetric unit. Eight intermolecular hydrogen bonds have donoracceptor distances in the range 2.602 (2)-3.289 (2) A, with angles in the range 137 (2)-177 (2). These generate a three-dimensional hydrogen-bond network. There is a single intramolecular hydrogen bond. There are six significant intermolecular CH- O interactions with H- O distances in the range 2.392.74 A, and C-H- O angles in the range 131-157. © 2000 International Union of Crystallography all rights reserved.

Original language	English
Pages (from-to)	1021-1023
Number of pages	3
Journal	Acta Crystallographica Section C: Crystal Structure Communications
Volume	56
Issue number	8
DOIs	https://doi.org/10.1107/s0108270100007083
State	Published - Aug 1 2000

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General Biochemistry, Genetics and Molecular Biology

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http://dx.doi.org/10.1107/S0108270100007083

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title = "Hydrogen bonding and C-H⋯O interactions in 3-(3-aminophthalimido)phthalic acid dihydrate",

abstract = "The title compound, C16H10N2O6-2H2O, crystallized in the centrosymmetric triclinic space group PI with one organic molecule and two water molecules as the asymmetric unit. Eight intermolecular hydrogen bonds have donoracceptor distances in the range 2.602 (2)-3.289 (2) A, with angles in the range 137 (2)-177 (2). These generate a three-dimensional hydrogen-bond network. There is a single intramolecular hydrogen bond. There are six significant intermolecular CH- O interactions with H- O distances in the range 2.392.74 A, and C-H- O angles in the range 131-157. {\textcopyright} 2000 International Union of Crystallography all rights reserved.",

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T1 - Hydrogen bonding and C-H⋯O interactions in 3-(3-aminophthalimido)phthalic acid dihydrate

AU - Amonette, Allison J.

AU - Gerkin, Roger E.

PY - 2000/8/1

Y1 - 2000/8/1

N2 - The title compound, C16H10N2O6-2H2O, crystallized in the centrosymmetric triclinic space group PI with one organic molecule and two water molecules as the asymmetric unit. Eight intermolecular hydrogen bonds have donoracceptor distances in the range 2.602 (2)-3.289 (2) A, with angles in the range 137 (2)-177 (2). These generate a three-dimensional hydrogen-bond network. There is a single intramolecular hydrogen bond. There are six significant intermolecular CH- O interactions with H- O distances in the range 2.392.74 A, and C-H- O angles in the range 131-157. © 2000 International Union of Crystallography all rights reserved.

AB - The title compound, C16H10N2O6-2H2O, crystallized in the centrosymmetric triclinic space group PI with one organic molecule and two water molecules as the asymmetric unit. Eight intermolecular hydrogen bonds have donoracceptor distances in the range 2.602 (2)-3.289 (2) A, with angles in the range 137 (2)-177 (2). These generate a three-dimensional hydrogen-bond network. There is a single intramolecular hydrogen bond. There are six significant intermolecular CH- O interactions with H- O distances in the range 2.392.74 A, and C-H- O angles in the range 131-157. © 2000 International Union of Crystallography all rights reserved.

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DO - 10.1107/s0108270100007083

M3 - Article

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JO - Acta Crystallographica Section C: Crystal Structure Communications

JF - Acta Crystallographica Section C: Crystal Structure Communications

IS - 8

ER -

Hydrogen bonding and C-H⋯O interactions in 3-(3-aminophthalimido)phthalic acid dihydrate

Abstract

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