Sonochemical Synthesis of Nanocrystalline Lead Chalcogenides: PbE (E = S, Se, Te)

Qing Li; Yi Ding; Mingwang Shao; Ji Wu; Guihua Yu; Yitai Qian

doi:10.1016/S0025-5408(02)01052-8

Sonochemical Synthesis of Nanocrystalline Lead Chalcogenides: PbE (E = S, Se, Te)

Qing Li, Yi Ding, Mingwang Shao, Ji Wu, Guihua Yu, Yitai Qian

Biochemistry, Chemistry & Physics

University of Science and Technology of China

Research output: Contribution to journal › Article › peer-review

72 Scopus citations

Abstract

Nanocrystalline lead chalcogenides PbE (E=S, Se, Te) were synthesized conveniently by the reaction of Pb(CH3COO)2·3H2O and elemental chalcogens in ethylenediamine (en) under ultrasonic irradiation. XRD and TEM techniques were employed to characterize the products. The solubility of chalcogen in en was found to be the key factor of the reaction. A three-step mechanism was proposed to account for the formation of the products.

Original language	American English
Journal	Materials Research Bulletin
Volume	38
DOIs	https://doi.org/10.1016/S0025-5408(02)01052-8
State	Published - Feb 20 2003

Disciplines

Chemistry

Keywords

Sonochemical
lead chalcogenides
nanocrystalline
synthesis

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title = "Sonochemical Synthesis of Nanocrystalline Lead Chalcogenides: PbE (E = S, Se, Te)",

abstract = " Nanocrystalline lead chalcogenides PbE (E=S, Se, Te) were synthesized conveniently by the reaction of Pb(CH3COO)2·3H2O and elemental chalcogens in ethylenediamine (en) under ultrasonic irradiation. XRD and TEM techniques were employed to characterize the products. The solubility of chalcogen in en was found to be the key factor of the reaction. A three-step mechanism was proposed to account for the formation of the products.",

keywords = "Sonochemical, lead chalcogenides, nanocrystalline, synthesis",

author = "Qing Li and Yi Ding and Mingwang Shao and Ji Wu and Guihua Yu and Yitai Qian",

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day = "20",

doi = "10.1016/S0025-5408(02)01052-8",

language = "American English",

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TY - JOUR

T1 - Sonochemical Synthesis of Nanocrystalline Lead Chalcogenides: PbE (E = S, Se, Te)

AU - Li, Qing

AU - Ding, Yi

AU - Shao, Mingwang

AU - Wu, Ji

AU - Yu, Guihua

AU - Qian, Yitai

PY - 2003/2/20

Y1 - 2003/2/20

N2 - Nanocrystalline lead chalcogenides PbE (E=S, Se, Te) were synthesized conveniently by the reaction of Pb(CH3COO)2·3H2O and elemental chalcogens in ethylenediamine (en) under ultrasonic irradiation. XRD and TEM techniques were employed to characterize the products. The solubility of chalcogen in en was found to be the key factor of the reaction. A three-step mechanism was proposed to account for the formation of the products.

AB - Nanocrystalline lead chalcogenides PbE (E=S, Se, Te) were synthesized conveniently by the reaction of Pb(CH3COO)2·3H2O and elemental chalcogens in ethylenediamine (en) under ultrasonic irradiation. XRD and TEM techniques were employed to characterize the products. The solubility of chalcogen in en was found to be the key factor of the reaction. A three-step mechanism was proposed to account for the formation of the products.

KW - Sonochemical

KW - lead chalcogenides

KW - nanocrystalline

KW - synthesis

UR - https://doi.org/10.1016/S0025-5408(02)01052-8

U2 - 10.1016/S0025-5408(02)01052-8

DO - 10.1016/S0025-5408(02)01052-8

M3 - Article

SN - 0025-5408

VL - 38

JO - Materials Research Bulletin

JF - Materials Research Bulletin

ER -

Sonochemical Synthesis of Nanocrystalline Lead Chalcogenides: PbE (E = S, Se, Te)

Abstract

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Keywords

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