Sonochemical synthesis of nanocrystalline lead chalcogenides: PbE (E = S, Se, Te)

Qing Li; Yi Ding; Mingwang Shao; Ji Wu; Guihua Yu; Yitai Qian

doi:10.1016/S0025-5408(02)01052-8

Sonochemical synthesis of nanocrystalline lead chalcogenides: PbE (E = S, Se, Te)

Qing Li
, Yi Ding
, Mingwang Shao
, Ji Wu
, Guihua Yu
, Yitai Qian

Biochemistry, Chemistry & Physics

University of Science and Technology of China

Research output: Contribution to journal › Article › peer-review

73 Scopus citations

Abstract

Nanocrystalline lead chalcogenides PbE (E = S, Se, Te) were synthesized conveniently by the reaction of Pb(CH₃COO)₂·3H₂O and elemental chalcogens in ethylenediamine (en) under ultrasonic irradiation. XRD and TEM techniques were employed to characterize the products. The solubility of chalcogen in en was found to be the key factor of the reaction. A three-step mechanism was proposed to account for the formation of the products.

Original language	English
Pages (from-to)	539-543
Number of pages	5
Journal	Materials Research Bulletin
Volume	38
Issue number	3
DOIs	https://doi.org/10.1016/S0025-5408(02)01052-8
State	Published - Feb 20 2003

Scopus Subject Areas

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

Keywords

Chalcogenides
Chemical synthesis
Nanostructures

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title = "Sonochemical synthesis of nanocrystalline lead chalcogenides: PbE (E = S, Se, Te)",

abstract = "Nanocrystalline lead chalcogenides PbE (E = S, Se, Te) were synthesized conveniently by the reaction of Pb(CH3COO)2·3H2O and elemental chalcogens in ethylenediamine (en) under ultrasonic irradiation. XRD and TEM techniques were employed to characterize the products. The solubility of chalcogen in en was found to be the key factor of the reaction. A three-step mechanism was proposed to account for the formation of the products.",

keywords = "Chalcogenides, Chemical synthesis, Nanostructures",

author = "Qing Li and Yi Ding and Mingwang Shao and Ji Wu and Guihua Yu and Yitai Qian",

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T1 - Sonochemical synthesis of nanocrystalline lead chalcogenides

T2 - PbE (E = S, Se, Te)

AU - Li, Qing

AU - Ding, Yi

AU - Shao, Mingwang

AU - Wu, Ji

AU - Yu, Guihua

AU - Qian, Yitai

PY - 2003/2/20

Y1 - 2003/2/20

N2 - Nanocrystalline lead chalcogenides PbE (E = S, Se, Te) were synthesized conveniently by the reaction of Pb(CH3COO)2·3H2O and elemental chalcogens in ethylenediamine (en) under ultrasonic irradiation. XRD and TEM techniques were employed to characterize the products. The solubility of chalcogen in en was found to be the key factor of the reaction. A three-step mechanism was proposed to account for the formation of the products.

AB - Nanocrystalline lead chalcogenides PbE (E = S, Se, Te) were synthesized conveniently by the reaction of Pb(CH3COO)2·3H2O and elemental chalcogens in ethylenediamine (en) under ultrasonic irradiation. XRD and TEM techniques were employed to characterize the products. The solubility of chalcogen in en was found to be the key factor of the reaction. A three-step mechanism was proposed to account for the formation of the products.

KW - Chalcogenides

KW - Chemical synthesis

KW - Nanostructures

UR - https://www.scopus.com/pages/publications/0037456566

U2 - 10.1016/S0025-5408(02)01052-8

DO - 10.1016/S0025-5408(02)01052-8

M3 - Article

SN - 0025-5408

VL - 38

SP - 539

EP - 543

JO - Materials Research Bulletin

JF - Materials Research Bulletin

IS - 3

ER -

Sonochemical synthesis of nanocrystalline lead chalcogenides: PbE (E = S, Se, Te)

Abstract

Scopus Subject Areas

Keywords

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