The synthesis of 1-(4-triethoxysilyl)phenyl-4,4,4-trifluoro-1,3- butanedione, a novel trialkoxysilane monomer for the preparation of functionalized sol-gel matrix materials

Christopher J. Peeples, Raghu Ram Earni, John C. DiCesare

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Abstract

The title compound, 1-(4-triethoxysilyl)phenyl)-4,4,4-trifluoro-1,3- butanedione, was synthesized in a three-step sequence starting from 2-(4-bromophenyl)propene. Containing both a trialkoxysilyl and a substituted 1,3-butanedione functional grouping within its structure, this new silane is a viable starting material for the preparation of functionalized sol-gel materials.

Original languageEnglish
Pages (from-to)2601-2607
Number of pages7
JournalMolecules
Volume13
Issue number10
DOIs
StatePublished - Oct 2008

Scopus Subject Areas

  • Analytical Chemistry
  • Chemistry (miscellaneous)
  • Molecular Medicine
  • Pharmaceutical Science
  • Drug Discovery
  • Physical and Theoretical Chemistry
  • Organic Chemistry

Keywords

  • 4,4,4-Trifluoro-1-phenyl-1,3-butanedione (4-TPB)
  • Molecular imprinting
  • Sol-gel
  • Trialkoxysilane

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